Chapter 12 Synthesis and Properties of Oxazole Heterocycles.
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The benefit of this lab was to acquaint oneself with the fundamentals of the Aldol Condensation reaction by demonstrating the synthesis of dibenzalacetone (trans, trans-1,5-Diphenyl-1,4-pentadien-3-one) through the aldol condensation of acetone with benzaldehyde. The synthesis began by using a strong base to generate the acetone enolate ion.
Background: A convenient synthesis of series of functionalized 5-(substituted phenyl)-3- phenylisoxazole (4a-f) has been carried out by using established p.
Thiophenes 5.1 Fiesselmann thiophene synthesis 5.2 Gewald aminothiophene synthesis 5.3 Hinsberg synthesis of thiophene derivatives 5.4 Paal thiophene synthesis Chapter 6. Oxazoles and Isoxazoles 6.1 Claisen isoxazole synthesis 6.2 Cornforth rearrangement 6.3 Erlenmeyer azlactone synthesis 6.4 Fischer oxazole synthesis 6.5 Meyers oxazoline method 6.6 Robinson.Gabriel synthesis 6.7 van Leusen.
Essay Experiments. enolate ions with carbonyl groups. One technique used was Doebner reaction and the other technique used was Claisen-Schmidt reaction. Therefore the aim of this experiment is to synthesize trans p-methoxycinnamic acid and to synthesize dibenzalacetone via an aldol condensation reaction between acetone and benzaldehyde.